1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene

Base Information

• Chemical Name: 1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene
• CAS No.: 400844-38-4
• Molecular Formula: C₄₂H₂₂F₂₀Fe
• Molecular Weight: 962.452
• Mol file: 400844-38-4.mol

Synonyms:

Chemical Property of 1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene

There total 1 articles about 1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

iron(II) bromide (7789-46-0) + sodium 1,2-bis(pentafluorophenyl)-4-tert-butylcyclopentadienide → 1,1',2,2'-tetrakis(pentafluorophenyl)-4,4'-di-tert-butylferrocene (400844-38-4)

Guidance literature:

In tetrahydrofuran; (inert atm.); stirring a soln. of sodium compd. and iron salt in THF at 25°C for 24 h; evapn., dissolving in benzene, filtration through neutral Al2O3, elutingwith hexanes, evapn., washing with pentane, drying in vac. recrystn. (h exanes); elem. anal.;

DOI:10.1016/S0022-328X(01)00878-6

upstream raw materials:

iron(II) bromide