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mer-Mo(H)Br(PhP(CH2CH2PPh2)2)(PMe2Ph)

Base Information
  • Chemical Name:mer-Mo(H)Br(PhP(CH2CH2PPh2)2)(PMe2Ph)
  • CAS No.:124715-54-4
  • Molecular Formula:C42H45BrMoP4
  • Molecular Weight:849.558
  • Hs Code.:
mer-Mo(H)Br(PhP(CH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)2)(PMe<sub>2</sub>Ph)

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Chemical Property of mer-Mo(H)Br(PhP(CH2CH2PPh2)2)(PMe2Ph)
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Technology Process of mer-Mo(H)Br(PhP(CH2CH2PPh2)2)(PMe2Ph)

There total 4 articles about mer-Mo(H)Br(PhP(CH2CH2PPh2)2)(PMe2Ph) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With HBr; In benzene; byproducts: N2; all manipulations under N2 or in vac.; condensing benzene and HBr successively onto the solid complex (-196°C), allowing to warm to room temp., stirring (15 h), color changing from red to green; filtering, adding pentane to the filtrate with rapid swirling, pptn., filtering, washing (pentane), drying (vac.); elem. anal.;
Guidance literature:
With HBr; In toluene; reacting complex with HBr in toluene (0.25 h, N2 atmosphere), adding pentane, pptn.;
Guidance literature:
With hydrogen bromide; In benzene; Mo:HBr=1:1, stirring (15 h);
DOI:10.1016/S0277-5387(00)80632-4
upstream raw materials:

fac-Mo(N2)(PhP(CH2CH2PPh2)2)(PMe2Ph)2

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