(tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)

Base Information

Chemical Name:(tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)
CAS No.:87607-81-6
Molecular Formula:C₄₉H₃₉FeN₄
Molecular Weight:739.722
Hs Code.:

(tetrakis(m-methylphenyl)porphyrin)Fe(CH<sub>3</sub>)

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Chemical Property of (tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)

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Technology Process of (tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)

There total 2 articles about (tetrakis(m-methylphenyl)porphyrin)Fe(CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 52155-49-4
C₂₀H₈N₄(C₆H₄CH₃)4FeCl

: 87607-81-6
(tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)

Guidance literature:: With methyl magnesium iodide; In toluene; 1 equiv of toluene soln. of MeMgI was added dropwise under vigorous stirring at 5-6°C under inert atmosphere to a soln. of Fe-complex intoluene, the mixt. was stirred for several min; hydrolyzed with Ar-satd. water, org. phase was washed until neutral, dried (MgSO4), evapd. in vacuo below 40°C, residue was chromd. overAl2O3 (benzene) in the dark, recrystd. from PhMe-heptane, dried for 24 h at 65°C/0.1 mmHg; elem. anal.;
DOI:10.1016/0022-328X(83)80109-0

Reference yield:

: 87612-88-2
Na⁽¹⁺⁾*Fe(C₂₀H₈N₄(C₆H₄CH₃)4)^(1-)=Na(Fe(C₂₀H₈N₄(C₆H₄CH₃)4))

: 87607-81-6
(tetrakis(m-methylphenyl)porphyrin)Fe(CH₃)

Guidance literature:: With methyl iodide; In diethyl ether; benzene; an excess of MeI was added dropwise with vigorous stirring to a soln. of Fe(I)-complex in 5:1 benzene/Et2O at ambient temp. under inert atmosphere, mixt. was stirred for several min (UV-vis monitoring); solvent was evapd., residue recrystd. from benzene-heptane; identified by the comparison of spectral data with that of authentic sample;
DOI:10.1016/0022-328X(83)80109-0