C₂₁H₃₂O₅Si

Base Information

Chemical Name:C₂₁H₃₂O₅Si
CAS No.:1388153-27-2
Molecular Formula:C₂₁H₃₂O₅Si
Molecular Weight:392.568
Hs Code.:

C<sub>21</sub>H<sub>32</sub>O<sub>5</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₂O₅Si

Chemical Property:

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Technology Process of C₂₁H₃₂O₅Si

There total 11 articles about C₂₁H₃₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388153-26-1
C₂₁H₃₄O₅Si

: 1388153-27-2
C₂₁H₃₂O₅Si

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 0 ℃; for 1h;
DOI:10.1021/ja305864z

Reference yield:

: 1388153-25-0
C₂₇H₄₈O₅Si₂

: 1388153-27-2
C₂₁H₃₂O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

2: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

With camphor-10-sulfonic acid; sulfur trioxide pyridine complex; triethylamine; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-88-2
C₁₄H₂₀O₄

: 1388153-27-2
C₂₁H₃₂O₅Si

Guidance literature:: Multi-step reaction with 10 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

4: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

5: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

6: tetrahydrofuran / 0.83 h / 20 °C

7: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

8: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

9: camphor-10-sulfonic acid / methanol; dichloromethane / 5 h / 0 °C

10: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C

With 1H-imidazole; 2,6-dimethylpyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; camphor-10-sulfonic acid; dihydrogen peroxide; sulfur trioxide pyridine complex; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z