Technology Process of C30H31ClN2O4
There total 7 articles about C30H31ClN2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: bromine / dichloromethane
2: Dichlorophenylphosphine; chlorine / Heating
3: isopropylmagnesium chloride lithium chloride complex / tetrahydrofuran / -20 °C
4: benzo[1,3,2]dioxaborole / benzene
5: perchloric acid
6: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide
7: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate / water; N,N-dimethyl acetamide
8: sodium hydroxide / water; tetrahydrofuran
With
bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium(0); perchloric acid; isopropylmagnesium chloride lithium chloride complex; bromine; chlorine; sodium carbonate; Dichlorophenylphosphine; sodium hydroxide; benzo[1,3,2]dioxaborole;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; benzene;
6: |Suzuki Coupling;
DOI:10.1021/ml500110j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: benzo[1,3,2]dioxaborole / benzene
2: perchloric acid
3: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide
4: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate / water; N,N-dimethyl acetamide
5: sodium hydroxide / water; tetrahydrofuran
With
bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium(0); perchloric acid; sodium carbonate; sodium hydroxide; benzo[1,3,2]dioxaborole;
In
tetrahydrofuran; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; benzene;
3: |Suzuki Coupling;
DOI:10.1021/ml500110j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide
2: tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate / water; N,N-dimethyl acetamide
3: sodium hydroxide / water; tetrahydrofuran
With
bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium(0); sodium carbonate; sodium hydroxide;
In
tetrahydrofuran; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
1: |Suzuki Coupling;
DOI:10.1021/ml500110j