(2-Amino-9H-fluoren-9-yl)methanol

Base Information

Chemical Name:(2-Amino-9H-fluoren-9-yl)methanol
CAS No.:162021-14-9
Molecular Formula:C₁₄H₁₃NO
Molecular Weight:211.263
Hs Code.:
DSSTox Substance ID:DTXSID90570242

Synonyms:(2-Amino-9H-fluoren-9-yl)methanol;162021-14-9;2-AMINO-9-HYDROXYMETHYLFLUORENE;9H-Fluorene-9-methanol, 2-amino-;9-hydroxymethyl-2-aminofluorene;MFCD24646252;SCHEMBL1230997;9-Hydroxymethyl-2-amino fluorene;9-Hydroxymethyl-2-amino-fluorene;DTXSID90570242;SYEYUWQQBFAPGD-UHFFFAOYSA-N;SC5062;AKOS027252271;SB78857;AS-54686;SY258681;CS-0155954

Suppliers and Price of (2-Amino-9H-fluoren-9-yl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Amino-9-hydroxymethylfluorene
500mg
$ 350.00

Crysdot
(2-Amino-9H-fluoren-9-yl)methanol 95+%
1g
$ 224.00

Crysdot
(2-Amino-9H-fluoren-9-yl)methanol 95+%
5g
$ 673.00

Ambeed
(2-Amino-9H-fluoren-9-yl)methanol 95%
5g
$ 614.00

Ambeed
(2-Amino-9H-fluoren-9-yl)methanol 95%
1g
$ 192.00

Ambeed
(2-Amino-9H-fluoren-9-yl)methanol 95%
250mg
$ 73.00

Ambeed
(2-Amino-9H-fluoren-9-yl)methanol 95%
100mg
$ 52.00

Total 3 raw suppliers

Chemical Property of (2-Amino-9H-fluoren-9-yl)methanol

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:211.099714038
Heavy Atom Count:16
Complexity:255

Purity/Quality:

95% ^*data from raw suppliers

2-Amino-9-hydroxymethylfluorene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C3=C(C=C(C=C3)N)C(C2=C1)CO
Uses 2-AMINO-9-HYDROXYMETHYLFLUORENE is a useful research chemical.

Technology Process of (2-Amino-9H-fluoren-9-yl)methanol

There total 5 articles about (2-Amino-9H-fluoren-9-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 141340-62-7
[2-(tert-butoxycarbonylamino)-9H-fluoren-9-yl]methanol

: 162021-14-9
9-hydroxymethyl-2-aminofluorene

Guidance literature:: [2-(tert-butoxycarbonylamino)-9H-fluoren-9-yl]methanol; With hydrogenchloride; water; In acetonitrile; for 0.75h; Heating / reflux;

With water; sodium carbonate; pH=9;

Reference yield:

: 153-78-6
2-aminofluorene

: 162021-14-9
9-hydroxymethyl-2-aminofluorene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 97 percent / aq. NaOH / dioxane / 25 °C

2.1: NaH / tetrahydrofuran

2.2: tetrahydrofuran

3.1: 13.0 g / NaBH₄ / methanol / 3.5 h

4.1: 87 percent / aq. HCl / dioxane / 0 - 25 °C

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1081/SCC-100000203

Reference yield:

: 141340-61-6
N-Boc-2-amino-fluorene

: 162021-14-9
9-hydroxymethyl-2-aminofluorene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran

1.2: tetrahydrofuran

2.1: 13.0 g / NaBH₄ / methanol / 3.5 h

3.1: 87 percent / aq. HCl / dioxane / 0 - 25 °C

With hydrogenchloride; sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; 1,4-dioxane; methanol;
DOI:10.1081/SCC-100000203