RBM1-75

Base Information

• Chemical Name: RBM1-75
• CAS No.: 1439377-30-6
• Molecular Formula: C₁₈H₃₉NO
• Molecular Weight: 285.514
• Mol file: 1439377-30-6.mol

Synonyms:

Chemical Property of RBM1-75

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of RBM1-75

There total 5 articles about RBM1-75 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C19H37NO2 (1439377-29-3) → RBM1-75 (1439377-30-6,196497-48-0)

Guidance literature:

With water; sodium hydroxide; In ethanol; for 2h; Reflux;

DOI:10.1021/jo400440z

Reference yield:

pentadec-1-yne (765-13-9) → RBM1-75 (1439377-30-6,196497-48-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: Schwartz's reagent / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice

1.2: 1 h / -40 - 20 °C / Inert atmosphere

2.1: potassium carbonate / methanol / 50 °C

3.1: hydrogen; 5wt.% Rh on activated alumina / ethyl acetate / 12 h / 20 °C / 760.05 Torr

4.1: water; sodium hydroxide / ethanol / 2 h / Reflux

With Schwartz's reagent; 5wt.% Rh on activated alumina; water; hydrogen; potassium carbonate; sodium hydroxide; In methanol; ethanol; dichloromethane; ethyl acetate;

DOI:10.1021/jo400440z

Reference yield:

C23H45NO3 → RBM1-75 (1439377-30-6,196497-48-0)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 50 °C

2: hydrogen; 5wt.% Rh on activated alumina / ethyl acetate / 12 h / 20 °C / 760.05 Torr

3: water; sodium hydroxide / ethanol / 2 h / Reflux

With 5wt.% Rh on activated alumina; water; hydrogen; potassium carbonate; sodium hydroxide; In methanol; ethanol; ethyl acetate;

DOI:10.1021/jo400440z

upstream raw materials:

C₁₉H₃₇NO₂

pentadec-1-yne

C₁₉H₃₅NO₂