Technology Process of C56H90N2O25
There total 8 articles about C56H90N2O25 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C52H88O24;
With
triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 1h;
Inert atmosphere;
imidazole-4-carboxylic acid chloride;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 24h;
Inert atmosphere;
DOI:10.5012/bkcs.2011.32.7.2193
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
1.2: 10 h / 20 °C / Inert atmosphere
2.1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
2.2: 24 h / 80 °C / Inert atmosphere
With
triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.7.2193
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium hydroxide / methanol; water / 4 h / Inert atmosphere; Reflux
1.2: Inert atmosphere; Reflux
2.1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 4 h / 20 °C / Inert atmosphere; Cooling with ice
3.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3.2: 10 h / 20 °C / Inert atmosphere
4.1: triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere
4.2: 24 h / 80 °C / Inert atmosphere
With
thionyl chloride; triethylamine; N,N-dimethyl-formamide; potassium hydroxide;
In
tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.7.2193
