C₃₀H₃₄O₂SSi

Base Information

Chemical Name:C₃₀H₃₄O₂SSi
CAS No.:82201-49-8
Molecular Formula:C₃₀H₃₄O₂SSi
Molecular Weight:486.75
Hs Code.:

C<sub>30</sub>H<sub>34</sub>O<sub>2</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₄O₂SSi

Chemical Property:

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Technology Process of C₃₀H₃₄O₂SSi

There total 9 articles about C₃₀H₃₄O₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32501-93-2
1-(Phenylsulfonyl)-2-(trimethylsilyl)acetylene

: 82201-49-8,87568-24-9
C₃₀H₃₄O₂SSi

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 5percent Pd-C / ethyl acetate; pyridine / 2585.7 Torr

2: 35 percent / toluene / 336 h / 160 °C

3: 1.) n-butyllithium / 1.) THF

With n-butyllithium; hydrogen; palladium on activated charcoal; In pyridine; ethyl acetate; toluene;
DOI:10.1016/S0040-4039(01)83002-1

Reference yield:

: 4837-01-8
1-bromo-2-phenylthioethane

: 82201-49-8,87568-24-9
C₃₀H₃₄O₂SSi

Guidance literature:: Multi-step reaction with 4 steps

1: sodium ethoxide / ethanol / 8 h / Heating

2: 78 percent / 30percent H₂O₂ / acetic acid / 1.) 70 deg C, 2.) reflux, 20 min

3: 98 percent / toluene / 168 h / 160 °C

4: 1.) n-BuLi / 1.) THF, hexane, 30 min, 2.) 30 min

With n-butyllithium; dihydrogen peroxide; sodium ethanolate; In ethanol; acetic acid; toluene;
DOI:10.1021/jo00173a039

Reference yield:

: 108-98-5
thiophenol

: 82201-49-8,87568-24-9
C₃₀H₃₄O₂SSi

Guidance literature:: Multi-step reaction with 5 steps

1: sodium ethoxide / 1.) ethanol, 45 min, 2.) 30 min

2: sodium ethoxide / ethanol / 8 h / Heating

3: 78 percent / 30percent H₂O₂ / acetic acid / 1.) 70 deg C, 2.) reflux, 20 min

4: 98 percent / toluene / 168 h / 160 °C

5: 1.) n-BuLi / 1.) THF, hexane, 30 min, 2.) 30 min

With n-butyllithium; dihydrogen peroxide; sodium ethanolate; In ethanol; acetic acid; toluene;
DOI:10.1021/jo00173a039