W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

Base Information

Chemical Name:W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)
CAS No.:501087-77-0
Molecular Formula:C₆₃H₅₁O₂PW
Molecular Weight:1054.92
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

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Technology Process of W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

There total 1 articles about W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: W(OC₆H(phenyl)4-2,3,5,6)2Cl₄

: 594-09-2
trimethylphosphane

: 501087-77-0
W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

Guidance literature:: With sodium amalgame; In toluene; N2; stirring toluene soln. of W compd. with excess (2.2-2.5 equiv.) of phosphine over sodium amalgame for 24 h at room temp.; decantation, filtration (Celite), evapn. in vac., recrystn. in benzene layered with hexane; elem. anal.;
DOI:10.1021/om030604m

Reference yield: 78.0%

: 501087-77-0
W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

: 20488-59-9
anti-2,2',4,4',6,6'-Hexamethylazobenzene

: W(OC₆H(phenyl)4-2,3,5,6)2(N(mesityl))

Guidance literature:: In benzene-d6; Irradiation (UV/VIS); N2; adding excess trans-azomesitylene to benzene-d6 soln. of W complex, irradn. with Hg-W lamp for 20 min, heating to 100°C for 5 min; elem. anal.;
DOI:10.1021/om030604m

Reference yield: 55.6%

: 230-17-1
benzo[c]cinnoline

: 501087-77-0
W(OC6H(phenyl)3-η6-phenyl)(OC6H(phenyl)4-2,3,5,6)(trimethylphosphine)

: 501087-79-2
W(OC₆H(phenyl)4-2,3,5,6)2(NC₁₂H₈N)(P(methyl)3)

Guidance literature:: In benzene; N2; adding excess benzo(c)cinnoline to benzene soln. of W complex, stirring for 2 h at room temp.; layering the soln. with hexane, drying the ppt. in vac.; elem. anal.;
DOI:10.1021/om030604m