Technology Process of 1-Hexanol, 6-(methylthio)-, 4-methylbenzenesulfonate
There total 3 articles about 1-Hexanol, 6-(methylthio)-, 4-methylbenzenesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylamine hydrochloride; triethylamine;
In
dichloromethane;
at 0 ℃;
for 1h;
DOI:10.1055/s-0031-1289552
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C
2: trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C
With
trimethylamine hydrochloride; potassium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1289552
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thiourea; potassium iodide / ethanol / 14 h / Reflux
1.2: 3 h / Reflux
2.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C
3.1: trimethylamine hydrochloride; triethylamine / dichloromethane / 1 h / 0 °C
With
trimethylamine hydrochloride; potassium carbonate; triethylamine; thiourea; potassium iodide;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1289552
