C₄₀H₄₇NO₁₃

Base Information

Chemical Name:C₄₀H₄₇NO₁₃
CAS No.:121846-22-8
Molecular Formula:C₄₀H₄₇NO₁₃
Molecular Weight:749.812
Hs Code.:

C<sub>40</sub>H<sub>47</sub>NO<sub>13</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₄₇NO₁₃

Chemical Property:

Purity/Quality:

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Technology Process of C₄₀H₄₇NO₁₃

There total 15 articles about C₄₀H₄₇NO₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 121846-22-8,121917-66-6
C₄₀H₄₇NO₁₃

Guidance literature:: Multi-step reaction with 11 steps

1: 96 percent / (i-Pr)2NEt

2: LiAlH₄ / diethyl ether / 0 °C

3: PCC, NaOAc

4: 45 percent / Ce(AcO)3-BF₃*Et₂O / toluene / -78 °C

5: NaBH₄, CeCl₃

7: Lemieux azidonitrating reagent

8: LiBr / acetonitrile

9: AgOTf / various solvent(s); tetrahydrofuran

10: Ph₃P / tetrahydrofuran

11: pyridine

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; Lemieux azidonitrating reagent; sodium acetate; silver trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; pyridinium chlorochromate; lithium bromide; boron trifluoride diethyl etherate; cerium(III) acetate; In tetrahydrofuran; diethyl ether; toluene; acetonitrile;
DOI:10.1021/ja00311a089

Reference yield:

: 33985-40-9
(3aR,4S,6R,6aR)-tetrahydro-6-methoxy-2,2-dimethylfuro-[3,4-d][1,3]dioxole-4-carbaldehyde

: 121846-22-8,121917-66-6
C₄₀H₄₇NO₁₃

Guidance literature:: Multi-step reaction with 14 steps

1: 85 percent / Eu(fod)3

2: 1.) O₃; 2.) H₂O₂, KOH / 1.) -78 deg C, CH₂Cl₂

4: 96 percent / (i-Pr)2NEt

5: LiAlH₄ / diethyl ether / 0 °C

6: PCC, NaOAc

7: 45 percent / Ce(AcO)3-BF₃*Et₂O / toluene / -78 °C

8: NaBH₄, CeCl₃

10: Lemieux azidonitrating reagent

11: LiBr / acetonitrile

12: AgOTf / various solvent(s); tetrahydrofuran

13: Ph₃P / tetrahydrofuran

14: pyridine

With pyridine; potassium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; Lemieux azidonitrating reagent; dihydrogen peroxide; sodium acetate; silver trifluoromethanesulfonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; pyridinium chlorochromate; lithium bromide; boron trifluoride diethyl etherate; cerium(III) acetate; Eu(fod)3; In tetrahydrofuran; diethyl ether; toluene; acetonitrile;
DOI:10.1021/ja00311a089

Reference yield:

: 99441-05-1
methyl 5,9-anhydro-6,8-dideoxy-2,3-O-(1-methylethylidene)-β-D-allo-non-8-enofuranosid-7-ulose

: 121846-22-8,121917-66-6
C₄₀H₄₇NO₁₃

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) O₃; 2.) H₂O₂, KOH / 1.) -78 deg C, CH₂Cl₂

3: 96 percent / (i-Pr)2NEt

4: LiAlH₄ / diethyl ether / 0 °C

5: PCC, NaOAc

6: 45 percent / Ce(AcO)3-BF₃*Et₂O / toluene / -78 °C

7: NaBH₄, CeCl₃

9: Lemieux azidonitrating reagent

10: LiBr / acetonitrile

11: AgOTf / various solvent(s); tetrahydrofuran

12: Ph₃P / tetrahydrofuran

13: pyridine

With pyridine; potassium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; Lemieux azidonitrating reagent; dihydrogen peroxide; sodium acetate; silver trifluoromethanesulfonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; pyridinium chlorochromate; lithium bromide; boron trifluoride diethyl etherate; cerium(III) acetate; In tetrahydrofuran; diethyl ether; toluene; acetonitrile;
DOI:10.1021/ja00311a089