C₂₉H₃₄BrNO₁₀

Base Information

Chemical Name:C₂₉H₃₄BrNO₁₀
CAS No.:496065-51-1
Molecular Formula:C₂₉H₃₄BrNO₁₀
Molecular Weight:636.494
Hs Code.:

C<sub>29</sub>H<sub>34</sub>BrNO<sub>10</sub>

Synonyms:

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Chemical Property of C₂₉H₃₄BrNO₁₀

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Technology Process of C₂₉H₃₄BrNO₁₀

There total 11 articles about C₂₉H₃₄BrNO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₄₁NO₁₃S

: 496065-51-1
C₂₉H₃₄BrNO₁₀

Guidance literature:: With potassium iodide; lithium bromide; In N,N-dimethyl-formamide; at 100 ℃; for 1h;
DOI:10.1139/v02-117

Reference yield:

: 96093-11-7
Methyl-2-azido-4,6-O-benzylidene-2-desoxy-β-D-galactopyranoside

: 496065-51-1
C₂₉H₃₄BrNO₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-iodosuccinimide; molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / -60 °C

1.2: 83 percent / trifluoromethanesulfonic acid / CH₂Cl₂ / 3 h / -60 - -30 °C

2.1: 94 percent / sodium methoxide / methanol / 2 h

3.1: 82 percent / dimethyl sulfoxide; acetic anhydride / 20 °C

4.1: 92 percent / L-selectride / tetrahydrofuran / 1 h / 0 °C

5.1: 102 mg / tetrahydrofuran; H₂O / 0.5 h

6.1: 79 percent / ammonium formate / 10 percent Pd/C / methanol / 1 h / Heating

7.1: 89 percent / 4-dimethylaminopyridine / pyridine / 18 h / 20 °C

8.1: 89 percent / H₂ / 10 percent Pd(OH)2/C / methanol / 18 h

9.1: pyridine / 3 h / 20 °C

10.1: LiBr; KI / dimethylformamide / 1 h / 100 °C

With pyridine; dmap; N-iodo-succinimide; 4 A molecular sieve; hydrogen; sodium methylate; ammonium formate; acetic anhydride; L-Selectride; dimethyl sulfoxide; potassium iodide; lithium bromide; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Zemplen transesterification;
DOI:10.1139/v02-117

Reference yield:

: phenyl 2-O-benzoyl-4-O-benzyl-3,6-dideoxy-1-thio-α,β-D-ribo-hexopyranoside

: 496065-51-1
C₂₉H₃₄BrNO₁₀

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-iodosuccinimide; molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / -60 °C

1.2: 83 percent / trifluoromethanesulfonic acid / CH₂Cl₂ / 3 h / -60 - -30 °C

2.1: 94 percent / sodium methoxide / methanol / 2 h

3.1: 82 percent / dimethyl sulfoxide; acetic anhydride / 20 °C

4.1: 92 percent / L-selectride / tetrahydrofuran / 1 h / 0 °C

5.1: 102 mg / tetrahydrofuran; H₂O / 0.5 h

6.1: 79 percent / ammonium formate / 10 percent Pd/C / methanol / 1 h / Heating

7.1: 89 percent / 4-dimethylaminopyridine / pyridine / 18 h / 20 °C

8.1: 89 percent / H₂ / 10 percent Pd(OH)2/C / methanol / 18 h

9.1: pyridine / 3 h / 20 °C

10.1: LiBr; KI / dimethylformamide / 1 h / 100 °C

With pyridine; dmap; N-iodo-succinimide; 4 A molecular sieve; hydrogen; sodium methylate; ammonium formate; acetic anhydride; L-Selectride; dimethyl sulfoxide; potassium iodide; lithium bromide; palladium dihydroxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Zemplen transesterification;
DOI:10.1139/v02-117