methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate

Base Information

Chemical Name:methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate
CAS No.:137847-70-2
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

methyl (3RS,1'R)-3-(methoxymethoxy)-4-<N-(1'-phenylethyl)carbamoyl>butyrate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate

Chemical Property:

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Technology Process of methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate

There total 4 articles about methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 112904-71-9
methyl hydrogen 3-(methoxymethoxy)glutarate

: 137847-70-2,137848-24-9
methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate

: 137847-69-9
methyl (3S,1'R)-3-acetoxy-4-butyrate

Guidance literature:: With thionyl chloride; triethylamine; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 112904-67-3
dimethyl 3-(methoxymethoxy)pentanedioate

: 137848-24-9
(S)-3-Methoxymethoxy-4-((R)-1-phenyl-ethylcarbamoyl)-butyric acid methyl ester

: 137847-70-2
(R)-3-Methoxymethoxy-4-((R)-1-phenyl-ethylcarbamoyl)-butyric acid methyl ester

Guidance literature:: With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; α-chymotrypsin; Multistep reaction; 1) pH=7.8 Na₂HPO₄ buffer in water, 23 deg C;
DOI:10.1016/S0040-4039(00)96663-2

Reference yield:

: 7250-55-7
dimethyl 3-hydroxypentanedioate

: 137847-70-2,137848-24-9
methyl (3RS,1'R)-3-(methoxymethoxy)-4-butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / Et₃N / diethyl ether / Ambient temperature

2: 65 percent / NaOH / H₂O / pig liver esterase

3: 78 percent / Et₃N, SOCl₂ / CH₂Cl₂ / 2 h / Ambient temperature

With sodium hydroxide; thionyl chloride; triethylamine; In diethyl ether; dichloromethane; water;