2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine

Base Information

• Chemical Name: 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine
• CAS No.: 166830-09-7
• Molecular Formula: C₃₁H₃₂N₂O₆
• Molecular Weight: 528.605

Synonyms:

Chemical Property of 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine

Chemical Property:

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Technology Process of 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine

There total 1 articles about 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',3'-dideoxy-3'-C-hydroxymethyl-β-D-erythro-pentopyranosyl thymine (166830-06-4) + mono-4-methoxytrityl chloride (14470-28-1) → 1-{(2R,4R,5S)-5-[(4-Methoxy-phenyl)-diphenyl-methoxy]-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-pyran-2-yl}-5-methyl-1H-pyrimidine-2,4-dione + 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine (166830-09-7)

Guidance literature:

With pyridine; dmap; at 80 ℃;

DOI:10.1016/0040-4020(95)00211-P

Reference yield: 37.0%

benzoic acid (65-85-0,8013-63-6) + 2',3'-dideoxy-3'-C--β-D-erythropentopyranosyl thymine (166830-09-7) → 1-{(R)-4-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-3,6-dihydro-2H-pyran-2-yl}-5-methyl-1H-pyrimidine-2,4-dione (166830-12-2) + 4'-O-benzoyl-2',3'-dideoxy-3'-C--α-L-threo-pentopyranosyl thymine

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; m-xylene;

DOI:10.1016/0040-4020(95)00211-P

upstream raw materials:

2',3'-dideoxy-3'-C-hydroxymethyl-β-D-erythro-pentopyranosyl thymine

mono-4-methoxytrityl chloride

Downstream raw materials:

1-{(R)-4-[(4-Methoxy-phenyl)-diphenyl-methoxymethyl]-3,6-dihydro-2H-pyran-2-yl}-5-methyl-1H-pyrimidine-2,4-dione

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