5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzophenantro<2,3-o>pentaphene trifluoromethanesulphonate

Base Information

• Chemical Name: 5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzo
• Molecular Formula: CF₃O₃S*C₄₃H₃₃O
• Molecular Weight: 714.805

Synonyms:

Chemical Property of 5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzo

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

There total 1 articles about 5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzophenantro<2,3-o>pentaphene trifluoromethanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

5,8,9,10-Tetrahydrobenz<α>anthracen-11(6H)-one (1470-04-8) + trifluorormethanesulfonic acid (1493-13-6) + 5,6,7,8-tetrahydro-10-(phenylmethylene)benzanthracen-11(10H)-one (1504-35-4) → 5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzophenantro<2,3-o>pentaphene trifluoromethanesulphonate (88065-22-9)

Guidance literature:

at 100 ℃; for 2.5h;

DOI:10.1039/P29830001455

Reference yield:

5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-oxoniabenzophenantro<2,3-o>pentaphene trifluoromethanesulphonate (88065-22-9) → 5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-azabenzophenantro<2,3-o>pentaphene (88065-23-0)

Guidance literature:

With ammonium hydroxide; acetic acid; Yield given. Multistep reaction; 1) CH₂Cl₂, 1 h; 2) CH₂Cl₂, 16 h;

DOI:10.1039/P29830001455

upstream raw materials:

5,8,9,10-Tetrahydrobenz<α>anthracen-11(6H)-one

trifluorormethanesulfonic acid

5,6,7,8-tetrahydro-10-(phenylmethylene)benzanthracen-11(10H)-one

Downstream raw materials:

5,6,8,9,11,12,14,15-octahydro-10-phenyl-21-azabenzophenantro<2,3-o>pentaphene

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