(3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

Base Information

Chemical Name:(3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester
CAS No.:167959-93-5
Molecular Formula:C₂₃H₃₁NO₃
Molecular Weight:369.504
Hs Code.:

(3S,4S,5S)-4-<N,N>-dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

Chemical Property:

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Technology Process of (3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

There total 2 articles about (3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 125655-07-4
(2S,3S)-2-(N,N-Dibenzylamino)-3-methylpentanal

: 167959-93-5
(3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) H₂O₂ / 1.) ethyl ether, dichloromethane, -78 deg C, 18 h, 2.) MeOH, room temperature, 45 min

2: aq. NaOH / tetrahydrofuran / 18 h / Ambient temperature

3: methanol; diethyl ether

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/S0040-4020(97)00215-9

Reference yield:

: 168038-85-5
(3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid tert-butyl thioester

: 167959-93-5
(3S,4S,5S)-4--dibenzylamino-3-hydroxy-5-methylheptanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / tetrahydrofuran / 18 h / Ambient temperature

2: methanol; diethyl ether

With sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1016/S0040-4020(97)00215-9