2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

Base Information

Chemical Name:2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one
CAS No.:141945-47-3
Molecular Formula:C₃₀H₂₄N₃O₃P
Molecular Weight:505.513
Hs Code.:

2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzo<ij>quinolizin-3-one

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Chemical Property of 2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

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Technology Process of 2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

There total 7 articles about 2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110216-66-5
1-azido-2-nitro-3-oxo-6,7-dihydro-3H,5H-benzoquinolizine

: 603-35-0
triphenylphosphine

: 141945-47-3
2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

Guidance literature:: In toluene; for 0.25h; Heating;

Reference yield:

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 141945-47-3
2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

Guidance literature:: Multi-step reaction with 7 steps

1: 60 percent / diphenyl ether / 5 h / Heating

2: 99 percent / NaOH / ethane-1,2-diol; H₂O / 1 h / Heating

3: 96 percent / 90percent aq. H₂SO₄ / 15 h / 140 °C

4: 89 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

5: 94 percent / triethylamine, phosphoryl chloride / 1 h / Heating

6: 89 percent / NaN₃ / various solvent(s) / 3 h / Ambient temperature

7: 80 percent / toluene / 0.25 h / Heating

With sodium hydroxide; sodium azide; sulfuric acid; nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In diphenylether; water; ethylene glycol; acetic acid; toluene;

Reference yield:

: 95594-15-3
9-hydroxy-8,11-dioxo-5,6,8,11-tetrahydro-4H-benzopyrano<2,3-b>quinolizine

: 141945-47-3
2-nitro-1-triphenylphosphoranylideneamino-6,7-dihydro-3H,5H-benzoquinolizin-3-one

Guidance literature:: Multi-step reaction with 6 steps

1: 99 percent / NaOH / ethane-1,2-diol; H₂O / 1 h / Heating

2: 96 percent / 90percent aq. H₂SO₄ / 15 h / 140 °C

3: 89 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

4: 94 percent / triethylamine, phosphoryl chloride / 1 h / Heating

5: 89 percent / NaN₃ / various solvent(s) / 3 h / Ambient temperature

6: 80 percent / toluene / 0.25 h / Heating

With sodium hydroxide; sodium azide; sulfuric acid; nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In water; ethylene glycol; acetic acid; toluene;