Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

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Chemical Name:Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester
CAS No.:87069-84-9
Molecular Formula:C₄₀H₅₇NO₁₁Se
Molecular Weight:806.853
Hs Code.:

Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

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Chemical Property of Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

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Technology Process of Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

There total 2 articles about Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73787-23-2
(+)-benzoylpedamide

: 87069-84-9
Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 12 h / Ambient temperature

2: 1) SOCl₂, pyridine; 2) NaBH₄ / 1) methylene dichloride, room temp., 2 h; 2) ethanol, -20 deg C, 30 min

With pyridine; sodium tetrahydroborate; thionyl chloride; In dichloromethane;
DOI:10.1016/S0040-4020(01)86075-0

Reference yield:

: 87045-89-4
(αS,2R,4R,5R,6R)-α-acetoxytetrahydro-2-methoxy-5,6-dimethyl-4-<(phenylseleno)methyl>-2H-pyran-2-acetic acid

: 85279-96-5
methyl benzoylpedimidate

: 87069-84-9
Benzoic acid (2R,4R,6S)-6-{(R)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

: 87045-90-7
Benzoic acid (2R,4R,6S)-6-{(S)-[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

Guidance literature:: With pyridine; sodium tetrahydroborate; thionyl chloride; Yield given. Multistep reaction; 1) methylene dichloride, room temp., 2 h; 2) ethanol, -20 deg C, 30 min;
DOI:10.1016/S0040-4020(01)86075-0

Reference yield:

: 87045-90-7,87069-84-9
Benzoic acid (2R,4R,6S)-6-{[(S)-2-acetoxy-2-((2R,4R,5R,6R)-2-methoxy-5,6-dimethyl-4-phenylselanylmethyl-tetrahydro-pyran-2-yl)-acetylamino]-methoxy-methyl}-2-((S)-2,3-dimethoxy-propyl)-3,3-dimethyl-tetrahydro-pyran-4-yl ester

: 87045-91-8,87069-85-0,111266-11-6,111266-12-7,111266-13-8,111319-48-3,130606-55-2
(αS,2R,4R,5R,6R)-N-<(S)-<(2S,4R,6R)-4-(benzoyloxy)-6-<(S)-2,3-dimethoxypropyl>-tetrahydro-5,5-dimethyl-2H-pyran-2-yl>methoxymethyl>-α-(benzoyloxy)tetrahydro-2-methoxy-5,6-dimethyl-4-<(phenylseleno)methyl>-2H-pyran-2-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LiOH; 2) DMAP / 1) MeOH, room temp., 3 h; 2) pyridine, room temp, 5 h

2: 23 percent / AcCl / 3 h / Ambient temperature

With dmap; lithium hydroxide; acetyl chloride;
DOI:10.1016/S0040-4020(01)86075-0