C₁₅H₁₆O₂

Base Information

Chemical Name:C₁₅H₁₆O₂
CAS No.:1318801-75-0
Molecular Formula:C₁₅H₁₆O₂
Molecular Weight:228.291
Hs Code.:

C<sub>15</sub>H<sub>16</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₅H₁₆O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₆O₂

Chemical Property:

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Technology Process of C₁₅H₁₆O₂

There total 6 articles about C₁₅H₁₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1318801-69-2
(Z)-4-phenethylhepta-4,6-diene-2,3-dione

: 1318801-74-9
C₁₅H₁₆O₂

: 1318801-75-0
C₁₅H₁₆O₂

Guidance literature:: With sodium hydride; malonic acid dimethyl ester; lithium chloride; yttrium(III) trifluoromethanesulfonate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja205440x

Reference yield:

: 1318801-84-1
(Z)-3-iodo-5-phenylpent-2-en-1-ol

: 1318801-75-0
C₁₅H₁₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: manganese(IV) oxide / dichloromethane / 12 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 °C / Inert atmosphere

3.2: 6 h / -78 °C / Inert atmosphere

3.3: -78 - 35 °C / Inert atmosphere

4.1: sodium hydride; malonic acid dimethyl ester; lithium chloride; yttrium(III) trifluoromethanesulfonate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; n-butyllithium; tert.-butyl lithium; sodium hydride; malonic acid dimethyl ester; lithium chloride; yttrium(III) trifluoromethanesulfonate; In tetrahydrofuran; hexane; dichloromethane; pentane; 4.1: Nazarov cyclization;
DOI:10.1021/ja205440x

Reference yield:

: 1318801-85-2
(Z)-3-iodo-5-phenylpent-2-enal

: 1318801-75-0
C₁₅H₁₆O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 °C / Inert atmosphere

2.2: 6 h / -78 °C / Inert atmosphere

2.3: -78 - 35 °C / Inert atmosphere

3.1: sodium hydride; malonic acid dimethyl ester; lithium chloride; yttrium(III) trifluoromethanesulfonate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With n-butyllithium; tert.-butyl lithium; sodium hydride; malonic acid dimethyl ester; lithium chloride; yttrium(III) trifluoromethanesulfonate; In tetrahydrofuran; hexane; pentane; 3.1: Nazarov cyclization;
DOI:10.1021/ja205440x