C₂₆H₃₅NO₄

Base Information

• Chemical Name: C₂₆H₃₅NO₄
• CAS No.: 190712-25-5
• Molecular Formula: C₂₆H₃₅NO₄
• Molecular Weight: 425.568
• Mol file: 190712-25-5.mol

Synonyms:

Chemical Property of C₂₆H₃₅NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₅NO₄

There total 4 articles about C₂₆H₃₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-6-benzyloxy-2-methyl-1-hexanol (188729-97-7) → C26H35NO4 (190712-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (COCl)2, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 0 °C

2: MgSO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With oxalyl dichloride; magnesium sulfate; dimethyl sulfoxide; triethylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)00522-4

Reference yield:

(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-methyl-hexan-1-ol (190712-19-7) → C26H35NO4 (190712-25-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) NaH / tetrahydrofuran; dimethylformamide / 99 h / 1.) - 15 deg C, 30 min; 2.) rt., 6 h

2: 94 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 2 h / Ambient temperature

3: (COCl)2, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 0 °C

4: MgSO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With oxalyl dichloride; tetrabutyl ammonium fluoride; sodium hydride; magnesium sulfate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(97)00522-4

Reference yield:

((S)-6-Benzyloxy-2-methyl-hexyloxy)-tert-butyl-diphenyl-silane (190712-20-0) → C26H35NO4 (190712-25-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 2 h / Ambient temperature

2: (COCl)2, DMSO, Et₃N / CH₂Cl₂ / 1 h / -78 - 0 °C

3: MgSO₄ / CH₂Cl₂ / 4 h / Ambient temperature

With oxalyl dichloride; tetrabutyl ammonium fluoride; magnesium sulfate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1016/S0040-4039(97)00522-4

upstream raw materials:

N-benzyl hydroxylalmine

(S)-6-benzyloxy-2-methyl-1-hexanol

(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-methyl-hexan-1-ol

((S)-6-Benzyloxy-2-methyl-hexyloxy)-tert-butyl-diphenyl-silane