C₃₁H₃₉NO₃

Base Information

• Chemical Name: C₃₁H₃₉NO₃
• CAS No.: 85535-02-0
• Molecular Formula: C₃₁H₃₉NO₃
• Molecular Weight: 473.656
• Mol file: 85535-02-0.mol

Synonyms:

Chemical Property of C₃₁H₃₉NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₃₁H₃₉NO₃

There total 1 articles about C₃₁H₃₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C31H37NO3*C4H6O6 (91653-24-6) → C31H39NO3 (85535-02-0)

Guidance literature:

With sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; Yield given. Multistep reaction; 1.) Et₂O, reflux, 18 h, 2.) Et₂O, H₂O;

DOI:10.1021/jm00361a019

Reference yield:

C31H39NO3 (85535-02-0) → C31H37NO3 (85535-08-6)

Guidance literature:

With TEA; trifluoroacetic anhydride; Yield given. Multistep reaction; 1.) Me₂SO, CH₂Cl₂, -60 deg C, 90 min, 2.) Me₂SO, CH₂Cl₂, from -60 deg C to RT;

DOI:10.1021/jm00361a019

Reference yield:

C31H39NO3 (85535-02-0) → C30H35NO3 (85535-12-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) trifluoroacetic anhydride, 2.) TEA / 1.) Me₂SO, CH₂Cl₂, -60 deg C, 90 min, 2.) Me₂SO, CH₂Cl₂, from -60 deg C to RT

2: 42 percent / 48percent HBr / 15 h / Heating

With TEA; hydrogen bromide; trifluoroacetic anhydride;

DOI:10.1021/jm00361a019

upstream raw materials:

C₃₁H₃₇NO₃*C₄H₆O₆

Downstream raw materials:

C₃₁H₃₇NO₃

C₃₀H₃₅NO₃