C₃₀H₂₈O₉

Base Information

• Chemical Name: C₃₀H₂₈O₉
• CAS No.: 75858-33-2
• Molecular Formula: C₃₀H₂₈O₉
• Molecular Weight: 532.547
• Mol file: 75858-33-2.mol

Synonyms:

Chemical Property of C₃₀H₂₈O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₈O₉

There total 13 articles about C₃₀H₂₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,6R,8S,9R)-8,9-Bis-benzyloxy-3,10-dioxa-bicyclo[4.3.1]decan-4-one (75858-31-0) → C30H28O9 (75858-33-2)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / Ambient temperature

2: trimethylsilyl iodide / CH₂Cl₂ / 2 h / Ambient temperature

3: pyridine, 4-dimethylaminopyridine

With pyridine; dmap; trimethylsilyl iodide; In methanol; dichloromethane;

Reference yield:

(E)-(5S,6S,7S)-5,6-Bis-benzyloxy-7,8-dihydroxy-oct-2-enoic acid methyl ester (75858-30-9) → C30H28O9 (75858-33-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 51 percent / 0.5 N sodium methoxide / methanol; toluene / 6 h / Heating

2: methanol / Ambient temperature

3: trimethylsilyl iodide / CH₂Cl₂ / 2 h / Ambient temperature

4: pyridine, 4-dimethylaminopyridine

With pyridine; dmap; trimethylsilyl iodide; sodium methylate; In methanol; dichloromethane; toluene;

Reference yield:

(E)-(5S,6R)-5,6-Bis-benzyloxy-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-hex-2-enoic acid methyl ester (75858-29-6) → C30H28O9 (75858-33-2)

Guidance literature:

Multi-step reaction with 5 steps

1: 88 percent / 80 percent aqueous acetic acid / 3 h / 55 °C

2: 51 percent / 0.5 N sodium methoxide / methanol; toluene / 6 h / Heating

3: methanol / Ambient temperature

4: trimethylsilyl iodide / CH₂Cl₂ / 2 h / Ambient temperature

5: pyridine, 4-dimethylaminopyridine

With pyridine; dmap; trimethylsilyl iodide; sodium methylate; acetic acid; In methanol; dichloromethane; toluene;

upstream raw materials:

benzoyl chloride

[4,6-dideoxy-6-(methoxycarbonyl)-D-gluco-β-C-pyranosyl] methanol

(1R,6R,8S,9R)-8,9-Bis-benzyloxy-3,10-dioxa-bicyclo[4.3.1]decan-4-one

(E)-(5S,6S,7S)-5,6-Bis-benzyloxy-7,8-dihydroxy-oct-2-enoic acid methyl ester