3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

Base Information

Chemical Name:3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate
CAS No.:123053-51-0
Molecular Formula:C₃₃H₅₂N₄O₆
Molecular Weight:600.799
Hs Code.:

Synonyms:

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Chemical Property of 3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

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Technology Process of 3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

There total 3 articles about 3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123053-50-9
(2S,5S)-2-tert-Butyl-5-(4-chloro-butyl)-3-methyl-4-oxo-imidazolidine-1-carboxylic acid tert-butyl ester

: 123053-51-0
3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / anhydrous NaI / various solvent(s) / 18 h / 110 °C

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 40 min: 2.) THF, hexane, -78 deg C warming to room temperature, 12 h

With sodium iodide; lithium diisopropyl amide; In various solvent(s);

Reference yield:

: 119838-38-9
(2S)-1-(tert-butyloxycarbonyl)-2-tert-butyl-3-methylimidazolidin-4-one

: 123053-51-0
3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium diisopropylamine (LDA) / 1.) THF, -78 deg C, 40 min: 2.) THF, -78 deg C warming to room temperature, 12 h

2: 78 percent / anhydrous NaI / various solvent(s) / 18 h / 110 °C

3: 1.) LDA / 1.) THF, hexane, -78 deg C, 40 min: 2.) THF, hexane, -78 deg C warming to room temperature, 12 h

With sodium iodide; lithium diisopropyl amide; In various solvent(s);

Reference yield:

: 119906-46-6,111610-19-6
(R)-2-t-butyl-1-carbobenzyloxy-3-methyl-4-imidazolidinone

: 123053-20-3
tert-butyl (2S,5S)-2-(tert-butyl)-5-(4-iodobutyl)-3-methyl-4-oxo-1-imidazolidinecarboxylate

: 123053-51-0
3-benzyl-3'-(tert-butyl) (2R,2'S,4R,4'S)-2,2'-di(tert-butyl)-1,1'-dimethyl-5,5'-dioxo-4,4'-(1,4-butanediyl)-bis(imidazolidine)-3,3'-dicarboxylate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 40 min: 2.) THF, hexane, -78 deg C warming to room temperature, 12 h;