4-O-allylacetophenone oxime benzoyl ester

Base Information

Chemical Name:4-O-allylacetophenone oxime benzoyl ester
CAS No.:1365655-56-6
Molecular Formula:C₁₈H₁₇NO₃
Molecular Weight:295.338
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-O-allylacetophenone oxime benzoyl ester

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Technology Process of 4-O-allylacetophenone oxime benzoyl ester

There total 2 articles about 4-O-allylacetophenone oxime benzoyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2089-30-7
C₁₁H₁₃NO₂

: 65-85-0,8013-63-6
benzoic acid

: 1365655-56-6
4-O-allylacetophenone oxime benzoyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 13h;
DOI:10.1021/jacs.9b06668 DOI:10.1021/jacs.9b06668

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1365655-56-6
4-O-allylacetophenone oxime benzoyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetonitrile / 5 h / 50 °C / Irradiation

1.2: 2 h / 90 °C

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 13 h / 0 - 20 °C

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jacs.9b06668 DOI:10.1021/jacs.9b06668