Boc-3-(Gly)2-OMe

Base Information

Chemical Name:Boc-3-(Gly)2-OMe
CAS No.:92072-71-4
Molecular Formula:C₅₂H₇₂N₈O₁₄
Molecular Weight:1033.19
Hs Code.:

Synonyms:

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Chemical Property of Boc-3-(Gly)2-OMe

Chemical Property:

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Technology Process of Boc-3-(Gly)2-OMe

There total 5 articles about Boc-3-(Gly)2-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92072-66-7
(S)-4-<3-(tert-butyloxycarbonyl)-5-oxo-4-oxazolidinyl>butanoic acid

: 92072-71-4
Boc-3-(Gly)2-OMe

Guidance literature:: Multi-step reaction with 5 steps

1: N-methylmorpholine / tetrahydrofuran / 0.5 h / -15 °C

2: N-methylmorpholine / tetrahydrofuran / 1.) -15 deg C, 1 h, 2.) RT, overnight

3: 98 percent / 1 N NaOH / methanol / 4 h / Ambient temperature

4: N-methylmorpholine / tetrahydrofuran / 0.33 h / -15 °C

5: N-methylmorpholine / tetrahydrofuran / 1.) -15 deg C, 1 h, 2.) RT, overnight

With 4-methyl-morpholine; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo00213a013

Reference yield:

: 92072-68-9
O-benzyl N-methyl-N^α-(tert-butyloxycarbonyl)-L-α-aminoadipo-δ-hydroxamate

: 92072-71-4
Boc-3-(Gly)2-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran / 0.33 h / -15 °C

2: N-methylmorpholine / tetrahydrofuran / 1.) -15 deg C, 1 h, 2.) RT, overnight

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1021/jo00213a013

Reference yield:

: (S)-4-(4-Isobutoxycarbonyloxy-4-oxo-butyl)-5-oxo-oxazolidine-3-carboxylic acid tert-butyl ester

: 92072-71-4
Boc-3-(Gly)2-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine / tetrahydrofuran / 1.) -15 deg C, 1 h, 2.) RT, overnight

2: 98 percent / 1 N NaOH / methanol / 4 h / Ambient temperature

3: N-methylmorpholine / tetrahydrofuran / 0.33 h / -15 °C

4: N-methylmorpholine / tetrahydrofuran / 1.) -15 deg C, 1 h, 2.) RT, overnight

With 4-methyl-morpholine; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo00213a013