2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

Base Information

Chemical Name:2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether
CAS No.:80692-14-4
Molecular Formula:C₁₃H₂₀ClNO
Molecular Weight:241.761
Hs Code.:

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Chemical Property of 2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

Chemical Property:

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Technology Process of 2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

There total 5 articles about 2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80692-10-0
1-[2-(2-Azido-propoxy)-2-methyl-propyl]-4-chloro-benzene

: 80692-14-4
2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Yield given; Heating;

Reference yield:

: 5468-97-3
1-(4-chlorophenyl)-2-methyl-2-propanol

: 80692-14-4
2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium hydride/dimethyl sulfoxide, triphenylmethane; 2.) / 1.) DMSO, 15-20 deg C; 2.) 15-20 deg C, 75 min

2: 1.) mercury(II) acetate; 2.) 0.5 M sodium borohydride, 3 M sodium hydroxide / 1.) water, THF, r.t.; 2.) THF, r.t., 10 min

3: 63 percent / pyridine / CH₂Cl₂ / 24 h / 0 °C

4: sodium azide / N,N-dimethyl-acetamide; H₂O / 4 h / 90 °C

5: lithium aluminium hydride / diethyl ether / 3 h / Heating

With pyridine; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium azide; triphenylmethane; mercury(II) diacetate; sodium hydride; dimethyl sulfoxide; In diethyl ether; dichloromethane; N,N-dimethyl acetamide; water;

Reference yield:

: 80692-07-5
3-(4-chlorophenyl)-2-methyl-2-propyl 2-propenyl ether

: 80692-14-4
2-aminopropyl 3-(4-chlorophenyl)-2-methyl-2-propyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) mercury(II) acetate; 2.) 0.5 M sodium borohydride, 3 M sodium hydroxide / 1.) water, THF, r.t.; 2.) THF, r.t., 10 min

2: 63 percent / pyridine / CH₂Cl₂ / 24 h / 0 °C

3: sodium azide / N,N-dimethyl-acetamide; H₂O / 4 h / 90 °C

4: lithium aluminium hydride / diethyl ether / 3 h / Heating

With pyridine; sodium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium azide; mercury(II) diacetate; In diethyl ether; dichloromethane; N,N-dimethyl acetamide; water;