((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

Base Information

Chemical Name:((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl
CAS No.:381219-40-5
Molecular Formula:C₆₃H₆₉ClN₃P₃Si₃Ti
Molecular Weight:1128.77
Hs Code.:

((CH<sub>3</sub>)3SiNC<sub>6</sub>H<sub>4</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3TiCl

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Chemical Property of ((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

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Technology Process of ((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

There total 1 articles about ((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 31011-57-1,112925-19-6,112925-18-5
tetrachlorobis(tetrahydrofuran)titanium(IV)

: 381219-43-8
(3-diphenylphosphanyl-phenyl)-trimethylsilanyl-amine

: 381219-40-5
((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

Guidance literature:: With n-BuLi; In diethyl ether; hexane; BuLi in hexane added dropwise to a stirred soln. of the ligand in Et2O at 0°C; stirred for 0.5 h at room temp.; cooled to 0°C; added dropwise to a stirred slurry of Ti complex in Et2O at 0°C; stirred at room temp. for 3 h; evapd., extd. with hot hexane, filtered through Celite, evapd. to dryness; elem. anal.;
DOI:10.1039/b105698k

Reference yield: 80.0%

: 57158-98-2
tris(norbornene)platinum⁽⁰⁾

: 381219-40-5
((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

: Pt((CH₃)3SiNC₆H₄P(C₆H₅)2)3TiCl

Guidance literature:: In toluene; toluene added to a stirred mixt. of solid Ti deriv. and Pt complex at -78°C; allowed to warm to room temp.; stirred at room temp. for 16 h; concnd. to 1 ml, cooled to -20°C, orange crystals sepd.; elem. anal.; X-ray detn.;
DOI:10.1039/b105698k