C₂₉H₃₁N₃O₅

Base Information

Chemical Name:C₂₉H₃₁N₃O₅
CAS No.:1273502-84-3
Molecular Formula:C₂₉H₃₁N₃O₅
Molecular Weight:501.582
Hs Code.:

C<sub>29</sub>H<sub>31</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₉H₃₁N₃O₅

Chemical Property:

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Technology Process of C₂₉H₃₁N₃O₅

There total 3 articles about C₂₉H₃₁N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915018-73-4
2-amino-1-(3,4-dihydroquinolin-1(2H)-yl)ethanone

: 17554-34-6
(2S)-2-[(benzyloxycarbonyl)amino]-3-(4-methoxyphenyl)propanoic acid

: 1273502-84-3
C₂₉H₃₁N₃O₅

Guidance literature:: 2-amino-1-(3,4-dihydroquinolin-1(2H)-yl)ethanone; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

(2S)-2-[(benzyloxycarbonyl)amino]-3-(4-methoxyphenyl)propanoic acid; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1039/c0ob00628a

Reference yield:

: benzyl [2-(3,4-dihydroquinolin-1(2H)-yl)-2-oxoethyl]carbamate

: 1273502-84-3
C₂₉H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / Inert atmosphere

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 0.17 h / 0 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1039/c0ob00628a

Reference yield:

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 1273502-84-3
C₂₉H₃₁N₃O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine; chloroformic acid ethyl ester / tetrahydrofuran / 0.17 h / -20 °C / Inert atmosphere

1.2: 0.25 h / -20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / Inert atmosphere

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3.2: 0.17 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; palladium 10% on activated carbon; hydrogen; chloroformic acid ethyl ester; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/c0ob00628a