{Cu(CH₃C(NOH)NNC₆H₅)(P(C₆H₅)3)2ClO₄}

Base Information

• Chemical Name: {Cu(CH₃C(NOH)NNC₆H₅)(P(C₆H₅)3)2ClO₄}
• CAS No.: 95686-31-0
• Molecular Formula: C₄₄H₃₉ClCuN₃O₅P₂
• Molecular Weight: 850.757
• Mol file: 95686-31-0.mol

Synonyms:

Chemical Property of {Cu(CH₃C(NOH)NNC₆H₅)(P(C₆H₅)3)2ClO₄}

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of {Cu(CH₃C(NOH)NNC₆H₅)(P(C₆H₅)3)2ClO₄}

There total 2 articles about {Cu(CH₃C(NOH)NNC₆H₅)(P(C₆H₅)3)2ClO₄} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

bis(phenylazoacetaldoxime)copper(I) perchlorate dihydrate → {Cu(CH3C(NOH)NNC6H5)(P(C6H5)3)2ClO4} (95686-31-0)

Guidance literature:

With triphenylphosphine; In acetone; to a soln. of complex in acetone PPh3 was added; absolute ethanol was added and the mixt. left in air for evapn., ppt. was awshed with benzene, dried in vac. over P4O10; elem. anal.;

DOI:10.1039/DT9850000159

Reference yield:

(phenylazoacetaldoximato)bis(triphenylphosphine)copper(I) → {Cu(CH3C(NOH)NNC6H5)(P(C6H5)3)2ClO4} (95686-31-0)

Guidance literature:

With perchloric acid; In acetone; to soln. of complex in acetone was added acetone contg. HClO4 slowly with stirring; absolute ethanol was added and the mixt. left for aerial evapn., ppt. was filtered off, washed with benzene and water, dried in vac.; elem. anal.;

DOI:10.1039/DT9850000159