t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate

Base Information

Chemical Name:t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate
CAS No.:130130-77-7
Molecular Formula:C₁₈H₂₉F₃O₃Si
Molecular Weight:378.507
Hs Code.:

t-Butyl 5β-<dimethyl(t-butyl)silyloxy>-6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate

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Technology Process of t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate

There total 7 articles about t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: Dimethyl(t-butyl)silyl trifluoromethanesulphonate

: 130130-75-5,130194-73-9,130194-79-5,130195-71-0
(1R,2S,3S,4S)-3-Trifluoromethyl-7-oxa-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid tert-butyl ester

: 130130-77-7,130130-86-8
t-Butyl 5β--6β-trifluoromethyl-cyclohexa-1,3-diene-carboxylate

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.75h;
DOI:10.1039/P19900001281

Reference yield: 77.0%

: 130130-76-6,130130-85-7
t-Butyl 5β-hydroxy-6α-trifluoromethylcyclohexa-1,3-diene-carboxylate

: 130130-77-7,130130-86-8
t-Butyl 5β--6α-trifluoromethyl-cyclohexa-1,3-diene carboxylate

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃;
DOI:10.1039/P19900001281

Reference yield:

: 136383-21-6,78762-71-7
trans-tert-butyl 4,4,4-trifluorocrotonate

: 130130-77-7,130130-86-8
t-Butyl 5β--6β-trifluoromethyl-cyclohexa-1,3-diene-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 h / 80 °C

2: 95 percent / 2,6-lutidine / CH₂Cl₂ / 0.75 h / 0 °C

With 2,6-dimethylpyridine; In dichloromethane;
DOI:10.1039/P19900001281