HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline)

Base Information

• Chemical Name: HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline)
• CAS No.: 1291082-05-7
• Molecular Formula: C₄₁H₂₄N₂O₉Os₃P₂
• Molecular Weight: 1321.2
• Mol file: 1291082-05-7.mol

Synonyms:

Chemical Property of HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline)

There total 1 articles about HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,1-Os3(CO)10(2,3-bis(diphenylphosphino)quinoxaline) (1291082-04-6,1291082-07-9) → HOs(CO)9[μ-2,3-PhP(η**(1)-C6H4)((C6H5)2P)quinoxaline) (1291082-05-7)

Guidance literature:

In toluene; byproducts: CO; Irradiation (UV/VIS); in Schlenk tube Os complex treated with toluene; satd. with CO, sealed, irradiated (366 nm) at room temp. for 3 d; concd. under vac.; residue chromatographed; recrystd. from hexane/benzene (1:1); elem. anal.;

DOI:10.1016/j.jorganchem.2011.01.019

upstream raw materials:

1,1-Os₃(CO)10(2,3-bis(diphenylphosphino)quinoxaline)