(TPP)Fe(ClO₄)2

Base Information

Chemical Name:(TPP)Fe(ClO₄)2
CAS No.:83435-87-4
Molecular Formula:C₄₄H₂₈N₄*2ClO₄*Fe
Molecular Weight:867.481
Hs Code.:

Synonyms:

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Chemical Property of (TPP)Fe(ClO₄)2

Chemical Property:

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Technology Process of (TPP)Fe(ClO₄)2

There total 4 articles about (TPP)Fe(ClO₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: iron(III) perchlorate nonahydrate

: 12582-61-5
((5,10,15,20-tetraphenylporphyrinato)iron(III))2O

: 135146-19-9,83435-87-4
5,10,15,20-tetraphenylporphyrin-iron(IV) diperchlorate

Guidance literature:: In dichloromethane; stirring; filtration; elem. anal.;
DOI:10.1021/ja00388a059

Reference yield:

: iron perchlorate hexahydrate

: 12582-61-5
μ-oxo-bis[α,β,γ,δ-tetraphenylporphinatoiron]

: 83435-87-4
(TPP)Fe(ClO₄)2

Guidance literature:: With perchloric acid; In perchloric acid; dichloromethane; (TPP)Fe(ClO4) generated from ((TPP)Fe)2O by shaking CH2Cl2 soln. with aq. 2 M HClO4, "acidic" (TPP)Fe(ClO4) soln. stirred while 10-fold excess Fe(ClO4)3*6H2O added over 4 h and mixt. stirred for 20 h; mixt. filtered, filtrate subjected to rotary evapn. with slow addn. heptane, crystals collected and dried under vac. for several hours;

Reference yield:

: 57715-43-2,59370-87-5
5,10,15,20-tetraphenylporphyrin iron(III) perchlorate

: iron(III) perchlorate

: 135146-19-9,83435-87-4
5,10,15,20-tetraphenylporphyrin-iron(IV) diperchlorate

: 5,10,15,20-tetraphenylporphyrin-iron(III) diperchlorate

Guidance literature:: In acetonitrile; Irradiation (UV/VIS); MeCN soln. of Fe(ClO4)3 mixed with Fe-complex in MeCN, irradiated at 396nm for 0.5-1 s at 21°C; Kinetics;