{Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ir₂(C₁₀H₁₆N₂)4}(B(C₆H₅)4)2

Base Information

• Chemical Name: {Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ir₂(C₁₀H₁₆N₂)4}(B(C₆H₅)4)2
• CAS No.: 110904-71-7
• Molecular Formula: 2C₂₄H₂₀B*C₄₀H₆₄Ir₂N₈
• Molecular Weight: 1679.91

Synonyms:

Chemical Property of {Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ir₂(C₁₀H₁₆N₂)4}(B(C₆H₅)4)2

Chemical Property:

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Technology Process of {Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ir₂(C₁₀H₁₆N₂)4}(B(C₆H₅)4)2

There total 1 articles about {Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4}⁽²⁺⁾*2B(C₆H₅)4^(1-)={Ir₂(C₁₀H₁₆N₂)4}(B(C₆H₅)4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro(1,5-cyclooctadiene)iridium(I) dimer + 2,5-dimethyl-2,5-diisocyanohexane + sodium tetraphenyl borate (143-66-8) → {Ir2((CH3)2C(NC)C2H4C(NC)(CH3)2)4}(2+)*2B(C6H5)4(1-)={Ir2(C10H16N2)4}(B(C6H5)4)2 (110904-71-7)

Guidance literature:

In dichloromethane; mixing stoich. quantities of ((C8H12)IrCl)2 and C10H16N2 in CH2Cl2; dissolving resulting solid in CH3OH and adding excess NaB(C6H5)4;; recrystn. of crude product from acetone;;

Reference yield:

{Ir2((CH3)2C(NC)C2H4C(NC)(CH3)2)4}(2+)*2B(C6H5)4(1-)={Ir2(C10H16N2)4}(B(C6H5)4)2 (110904-71-7) + sodium tetraphenyl borate (143-66-8) → [Ir2((CH2C(CH3)2NC)2)4Cl2](2+)*2B(C6H5)4(1-)=[Ir2((CH2C(CH3)2NC)2)4Cl2][B(C6H5)4]2

Guidance literature:

With Cl₂; In acetonitrile; MeCN soln. of educt titrated with MeCN soln. of Cl2 until the blue color disappeared; evapd., solid slurried in MeOH, filtered, solid collected, soln. of NaBPh4 added to filtrate, ppt. filtered off, combined solids crystd. from MeCN;

DOI:10.1021/ja00312a021

Reference yield:

{Ir2((CH3)2C(NC)C2H4C(NC)(CH3)2)4}(2+)*2B(C6H5)4(1-)={Ir2(C10H16N2)4}(B(C6H5)4)2 (110904-71-7) + sodium tetraphenyl borate (143-66-8) → [Ir2((CH2C(CH3)2NC)2)4I2](2+)*2B(C6H5)4(1-)=[Ir2((CH2C(CH3)2NC)2)4I2][B(C6H5)4]2

Guidance literature:

With I₂; In acetonitrile; MeCN soln. of educt titrated with MeCN soln. of I2 until the blue colordisappeared; evapd., solid slurried in MeOH, filtered, solid collected, soln. of NaBPh4 added to filtrate, ppt. filtered off, combined solids crystd. from MeCN;

DOI:10.1021/ja00312a021

upstream raw materials:

sodium tetraphenyl borate

Downstream raw materials:

{Ir₂((CH₃)2C(NC)C₂H₄C(NC)(CH₃)2)4I₂}⁽²⁺⁾*2B(C₆H₅)4^(1-)*1.5(CH₃)2CO={Ir₂(C₁₀H₁₆N₂)4I₂}(B(C₆H₅)4)2*1.5(CH₃)2CO

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