Technology Process of C19H34N4O
There total 5 articles about C19H34N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; water;
at 20 ℃;
for 16h;
DOI:10.1016/j.bmcl.2011.06.092
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / 40 h / 60 °C
2: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; water / 16 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2011.06.092
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tris(acetoxy)borohydride / methanol / 16 h / 20 °C
2: trifluoroacetic acid / dichloromethane / 20 °C
3: potassium carbonate / acetone / 40 h / 60 °C
4: palladium 10% on activated carbon; hydrogen / ethanol / 2 h / 20 °C
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; water / 16 h / 20 °C
With
palladium 10% on activated carbon; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
methanol; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2011.06.092
