C₆₈H₈₆O₄S₄

Base Information

Chemical Name:C₆₈H₈₆O₄S₄
CAS No.:96854-60-3
Molecular Formula:C₆₈H₈₆O₄S₄
Molecular Weight:1095.69
Hs Code.:

C<sub>68</sub>H<sub>86</sub>O<sub>4</sub>S<sub>4</sub>

Synonyms:

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Chemical Property of C₆₈H₈₆O₄S₄

Chemical Property:

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Technology Process of C₆₈H₈₆O₄S₄

There total 17 articles about C₆₈H₈₆O₄S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64670-06-0
methyl (+/-)-8-bromo-3-oxooctanoate

: 96854-60-3
C₆₈H₈₆O₄S₄

Guidance literature:: Multi-step reaction with 8 steps

1: NaBH₄ / methanol / 1 h / 0 °C

2: 1 M DIBAL / tetrahydrofuran; hexane / 1 h / -20 °C

3: p-TsOH / dioxane / 1 h / 20 °C

4: 1.) Mg, I₂ / 1.) THF; 2.) THF

5: pyridinium dichromate / dimethylformamide

6: BF₃*etherate / CH₂Cl₂

7: 4-dimethylaminopyridine, triethylamine / CH₂Cl₂

8: NaH, Bu₄NI / tetrahydrofuran

With dmap; sodium tetrahydroborate; dipyridinium dichromate; boron trifluoride diethyl etherate; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00021369.1985.10866672

Reference yield:

: 96854-42-1
8-Bromo-octane-1,3-diol

: 96854-60-3
C₆₈H₈₆O₄S₄

Guidance literature:: Multi-step reaction with 6 steps

1: p-TsOH / dioxane / 1 h / 20 °C

2: 1.) Mg, I₂ / 1.) THF; 2.) THF

3: pyridinium dichromate / dimethylformamide

4: BF₃*etherate / CH₂Cl₂

5: 4-dimethylaminopyridine, triethylamine / CH₂Cl₂

6: NaH, Bu₄NI / tetrahydrofuran

With dmap; dipyridinium dichromate; boron trifluoride diethyl etherate; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; magnesium; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00021369.1985.10866672

Reference yield:

: 108383-14-8
(+/-)-8-bromo-1,3-dihydroxyoctane-1,3-isopropylideneacetal

: 96854-60-3
C₆₈H₈₆O₄S₄

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Mg, I₂ / 1.) THF; 2.) THF

2: pyridinium dichromate / dimethylformamide

3: BF₃*etherate / CH₂Cl₂

4: 4-dimethylaminopyridine, triethylamine / CH₂Cl₂

5: NaH, Bu₄NI / tetrahydrofuran

With dmap; dipyridinium dichromate; boron trifluoride diethyl etherate; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00021369.1985.10866672