4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

Base Information

Chemical Name:4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone
CAS No.:133363-73-2
Molecular Formula:C₁₈H₁₅NO₃S
Molecular Weight:325.388
Hs Code.:

Synonyms:

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Chemical Property of 4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

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Technology Process of 4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

There total 8 articles about 4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52562-18-2
2-(prop-1-en-1-yl)aniline

: 133363-73-2
4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / pyridine / 16 h / Ambient temperature

2: 1) NaH / 1) benzene, r.t., 30 min, 2) benzene, refluxed, 2 h

3: 87 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.17 h / Ambient temperature

4: 94 percent / trifluoroacetic acid, trifluoroacetic acid anhydride / 1.5 h / 0 °C

5: m-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

6: NaHCO₃ / toluene / 4.5 h / Heating

With pyridine; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; toluene;
DOI:10.1248/cpb.38.3331

Reference yield:

: 51315-71-0
N--p-toluenesulfonamide

: 133363-73-2
4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

Guidance literature:: Multi-step reaction with 5 steps

1: 1) NaH / 1) benzene, r.t., 30 min, 2) benzene, refluxed, 2 h

2: 87 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.17 h / Ambient temperature

3: 94 percent / trifluoroacetic acid, trifluoroacetic acid anhydride / 1.5 h / 0 °C

4: m-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

5: NaHCO₃ / toluene / 4.5 h / Heating

With sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; toluene;
DOI:10.1248/cpb.38.3331

Reference yield:

: 133363-69-6,133363-82-3
N-<2-(methylsulfinyl)acetyl>-N--p-toluenesulfonamide

: 133363-73-2
4-ethenyl-1-(p-toluenesulfonyl)-2(1H)-quinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / trifluoroacetic acid, trifluoroacetic acid anhydride / 1.5 h / 0 °C

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

3: NaHCO₃ / toluene / 4.5 h / Heating

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; toluene;
DOI:10.1248/cpb.38.3331