Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)]PF₆

Base Information

• Chemical Name: Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)]PF₆
• CAS No.: 1365904-38-6
• Molecular Formula: C₅₆H₄₇N₂P₄Pt*F₆P
• Molecular Weight: 1211.94

Synonyms:

Chemical Property of Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)]PF₆

Chemical Property:

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Technology Process of Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)]PF₆

There total 1 articles about Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(C₆H₅)3)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

tetrakis(triphenylphosphine)platinum (14221-02-4) + C38H32N2P3(1+)*F6P(1-) → Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)(1+)*PF6(1-)=[Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)]PF6 (1365904-38-6)

Guidance literature:

In tetrahydrofuran; Schlenk technique; Pt complex added to suspn. of N-heterocyclic phosphenium ligand in THF, mixt. stirred at ambient temp. for 1 h; evapn. under vac., residue washed with Et2O, dissolved in THF, diffusionof Et2O vapor into soln.; elem. anal.;

DOI:10.1021/ic202581v

Reference yield: 95.6%

Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)(1+)*PF6(1-)=[Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)]PF6 (1365904-38-6) + trimethylphosphane (594-09-2) → Pt(P(NC6H4P(C6H5)2)2C2H4)(P(CH3)3)(1+)*PF6(1-)=[Pt(P(NC6H4P(C6H5)2)2C2H4)(P(CH3)3)]PF6 (1365904-41-1)

Guidance literature:

In dichloromethane; Schlenk technique; Me3P added to soln. of Pt complex in CH2Cl2, mixt. stirred for 12 h; evapn.; elem. anal.;

DOI:10.1021/ic202581v

Reference yield: 95.1%

Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)(1+)*PF6(1-)=[Pt(P(NC6H4P(C6H5)2)2C2H4)(P(C6H5)3)]PF6 (1365904-38-6) + phenol (108-95-2,27073-41-2) → PtH(P(C6H5)3)(POC6H5N2C2H4(C6H4P(C6H5)2)2)(1+)*PF6(1-)=PtH(P(C6H5)3)(POC6H5N2C2H4(C6H4P(C6H5)2)2)(PF6) (1391951-02-2)

Guidance literature:

In dichloromethane; (Schlenk, glovebox) phenol was added to a soln. of complex in CH2Cl2, heated in a sealed vessel in an oil bath at 60°C for 2 days; volatiles were removed in vac.; elem. anal.;

DOI:10.1039/c2dt30455d

upstream raw materials:

tetrakis(triphenylphosphine)platinum

Downstream raw materials:

[PtI₂(CH₃P(NC₆H₄P(C₆H₅)2)2C₂H₄)]

PtI(CH₃P(NC₆H₄P(C₆H₅)2)2C₂H₄)⁽¹⁺⁾*PF₆^(1-)=[PtI(CH₃P(NC₆H₄P(C₆H₅)2)2C₂H₄)]PF₆

Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(CH₃)3)⁽¹⁺⁾*PF₆^(1-)=[Pt(P(NC₆H₄P(C₆H₅)2)2C₂H₄)(P(CH₃)3)]PF₆

PtH(P(C₆H₅)3)(POC₆H₅N₂C₂H₄(C₆H₄P(C₆H₅)2)2)⁽¹⁺⁾*PF₆^(1-)=PtH(P(C₆H₅)3)(POC₆H₅N₂C₂H₄(C₆H₄P(C₆H₅)2)2)(PF₆)

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