N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

Base Information

Chemical Name:N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide
CAS No.:52553-07-8
Molecular Formula:C₃₀H₂₈N₄O₆
Molecular Weight:540.576
Hs Code.:

<i>N</i>-((4<i>R</i>)-2,2-dimethyl-(3a<i>t</i>,13a<i>t</i>)-4,5,13,13a-tetrahydro-3a<i>H</i>-4<i>r</i>,13<i>c</i>-epioxido-[1,3]dioxolo[4,5-<i>e</i>]pyrimido[5',4':4,5]pyrrolo[2,1-<i>b</i>][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

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Suppliers and Price of N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

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Chemical Property of N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

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Technology Process of N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

There total 3 articles about N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16739-75-6
((3aR,4R,6R,6aR)-6-(4-amino-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 52553-07-8
N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: NBS / acetone; CH₂Cl₂

2: H₂, NaOAc / Pd-C / ethanol

3: pyridine

With N-Bromosuccinimide; hydrogen; sodium acetate; palladium on activated charcoal; In pyridine; ethanol; dichloromethane; acetone;
DOI:10.1246/bcsj.47.417

Reference yield:

: 51385-16-1
(4R)-7-bromo-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-ylamine

: 52553-07-8
N-((4R)-2,2-dimethyl-(3at,13at)-4,5,13,13a-tetrahydro-3aH-4r,13c-epioxido-[1,3]dioxolo[4,5-e]pyrimido[5',4':4,5]pyrrolo[2,1-b][1,3]oxazocin-8-yl)-4,4'-dimethyl-dibenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, NaOAc / Pd-C / ethanol

2: pyridine

With hydrogen; sodium acetate; palladium on activated charcoal; In pyridine; ethanol;
DOI:10.1246/bcsj.47.417