hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

Base Information

Chemical Name:hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate
CAS No.:87635-52-7
Molecular Formula:C₁₀H₄O₈*CoH₁₂O₆
Molecular Weight:419.222
Hs Code.:

Synonyms:

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Chemical Property of hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

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Technology Process of hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

There total 4 articles about hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: cobalt(II) chloride hexahydrate

: 7732-18-5
water

: 6151-22-0,76532-02-0,83454-02-8
1,2,4,5-benzenetetracarboxylic acid dihydrate

: 87635-52-7
hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

Guidance literature:: With (NH₄)Mo₇O₂₄*6H₂O; In water; High Pressure; mixt. of Co salt, C10H10O10, ammonium molybdate and H2O in molar ratio 1:2:1:900 heated in autoclave at 160°C for 3 d under static conditions and filling vol. of 75 %, cooled to room temp.; washed (distd. H2O, EtOH), dried in air at room temp.; elem. anal.; detd. by TG/DTA;
DOI:10.1134/S1070328407070019

Reference yield:

: cobalt(II) sulfate

: 89-05-4
1,2,4,5-benzenetetracarboxylic acid

: 87635-52-7
hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

Guidance literature:: With BaCl₂; KOH; In water; byproducts: KCl, BaSO4; aq. soln. of BaCl2 added to aq. soln. of C6H2(COOH)4 and of KOH, suspn. stirred at room temp. for 2 h, aq. soln. of CoSO4 added to mixt., and warmed to 80°C for few min, stirred at room temp. for 15 h, filtered; DMF added to filtrate;
DOI:10.1016/S0020-1693(00)00086-4

Reference yield:

: cobalt (II) perchlorate hexahydrate

: 89-05-4
1,2,4,5-benzenetetracarboxylic acid

: 87635-52-7
hexaaquacobalt(II) dihydrogen 1,2,4,5-benzenetetracarboxylate

Guidance literature:: In methanol; water; mixing of (Co(H2O)6)(ClO4)2 and (COOH)4C6H2 in 1:1 molar ratio in methanol/water, heating to 60°C with stirring for 1 h; filtration, slow evapn. of filtrate at room temp. within a week; elem. anal.;
DOI:10.1016/S0022-2860(02)00046-7