Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester

Base Information

• Chemical Name: Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester
• CAS No.: 81793-95-5
• Molecular Formula: C₄₆H₅₁Br₃NO₁₆P
• Molecular Weight: 1144.59

Synonyms:

Chemical Property of Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester

Chemical Property:

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Technology Process of Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester

There total 1 articles about Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2,2-tribromoethyl phosphoranilidochloridate (71260-65-6) + Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-hydroxy-propoxy}-tetrahydro-pyran-3-yl ester (81794-03-8) → Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester (81793-95-5)

Guidance literature:

With 1-methyl-1H-imidazole; In acetonitrile; molecular sieves (4 Angstroem);

DOI:10.1016/S0040-4039(01)83029-X

Reference yield:

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-3-yl ester (81793-95-5) → Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-{3-hydroxy-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-4-yl ester (81793-96-6)

Guidance literature:

In acetic acid; at 20 ℃; for 0.5h;

DOI:10.1016/S0040-4039(01)83029-X

upstream raw materials:

2,2,2-tribromoethyl phosphoranilidochloridate

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-hydroxy-propoxy}-tetrahydro-pyran-3-yl ester

Downstream raw materials:

Acetic acid (2R,3R,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-{3-hydroxy-2-[phenylamino-(2,2,2-tribromo-ethoxy)-phosphoryloxy]-propoxy}-tetrahydro-pyran-4-yl ester

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