Sb₅(C₆H₃-2,6-(CH₂NMe₂)2)3

Base Information

• Chemical Name: Sb₅(C₆H₃-2,6-(CH₂NMe₂)2)3
• CAS No.: 1024021-17-7
• Molecular Formula: C₃₆H₅₇N₆Sb₅
• Molecular Weight: 1182.64
• Mol file: 1024021-17-7.mol

Synonyms:

Chemical Property of Sb₅(C₆H₃-2,6-(CH₂NMe₂)2)3

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of Sb₅(C₆H₃-2,6-(CH₂NMe₂)2)3

There total 1 articles about Sb₅(C₆H₃-2,6-(CH₂NMe₂)2)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

Sb(C6H3-2,6-(CH2NMe2)2)Cl2 (144501-67-7) → Sb5(C6H3-2,6-(CH2NMe2)2)3 (1024021-17-7) + Sb4(C6H3-2,6-(CH2NMe2)2)4 (1023697-62-2)

Guidance literature:

With K[B(isobutyl)3H]; In tetrahydrofuran; byproducts: hydrogen, C6H4(CH2N(CH3)2)2; addn. of soln. of K(B(i-Bu)3H) (2 equiv.) in THF to precooled (0°C) soln. of SbCl2(C6H3(CH2NMe2)2) in THF; warming to room temp.; stirring for 10 min; evolution of H2; evapn. of solvent in vac., extn. with hexane; filtration, concn.; crystn. for 5 h; filtration, washing with hexane;

DOI:10.1021/om800227m

upstream raw materials:

Sb(C₆H₃-2,6-(CH₂NMe₂)2)Cl₂