trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate

Base Information

Chemical Name:trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate
CAS No.:64552-65-4
Molecular Formula:C₄₀H₃₅ClCoN₇O₆S*H₂O
Molecular Weight:854.289
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate

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Technology Process of trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate

There total 2 articles about trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: cobalt(II) chloride hexahydrate

: 522-34-9
Diphenylglyoxime

: 16803-97-7
p-aminobenzenesulphonamido-4-aniline

: 64552-65-4
trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate

Guidance literature:: With oxygen; In butan-1-ol; mixt. of Co-salt and dioxime in solvent oxidn. by atmospheric oxygen (5 h, 70°C) until complete dissoln., aniline derivate addn., pptn. after 30 min; ppt. filtration off, washing (water, ethanol, ether); elem. anal.; thermogravimetric anal.;

Reference yield:

: 36795-68-3
trans-chlorobis(diphenylgyloximato)aquocobalt(III)

: 522-34-9
Diphenylglyoxime

: 64552-65-4
trans-chlorobis(diphenylglyoximato)(p.aminobenzenesulphonamido-4-aniline)cobalt(III) monohydrate

Guidance literature:: In acetone; heating suspn. of Co-complex and org. ligand (molar ratio 1:1, 70°C, 15 min), crystn. on ether addn.; elem. anal.; thermogravimetric anal.;