1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on

Base Information

• Chemical Name: 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on
• CAS No.: 38627-60-0
• Molecular Formula: C₂₅H₁₈O₃
• Molecular Weight: 366.416

Synonyms:

Chemical Property of 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on

Chemical Property:

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Technology Process of 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on

There total 3 articles about 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-Dimethoxy-1,3-diphenyl-2,3-dihydro-1H-cyclopenta[b]naphthalene-1,3-diol (38627-59-7) → 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on (38627-60-0)

Guidance literature:

With hydrogenchloride; In acetic acid; at 20 ℃; for 168h;

DOI:10.1039/P19720002722

Reference yield:

2,2-Dimethoxybenzinden-1,3-dion (38627-58-6) → 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on (38627-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; benzene

2: aq. HCl / acetic acid / 168 h / 20 °C

With hydrogenchloride; In diethyl ether; acetic acid; benzene;

DOI:10.1039/P19720002722

Reference yield:

phenylmagnesium bromide → 1,3-Dihydro-1,3-dihydroxy-1,3-diphenylbenzinden-2-on (38627-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; benzene

2: aq. HCl / acetic acid / 168 h / 20 °C

With hydrogenchloride; In diethyl ether; acetic acid; benzene;

DOI:10.1039/P19720002722

upstream raw materials:

2,2-Dimethoxy-1,3-diphenyl-2,3-dihydro-1H-cyclopenta[b]naphthalene-1,3-diol

2,2-Dimethoxybenzinden-1,3-dion

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