(S)-N-benzyl-4-acetoxy-cis-7-decenamide

Base Information

• Chemical Name: (S)-N-benzyl-4-acetoxy-cis-7-decenamide
• CAS No.: 1163138-26-8
• Molecular Formula: C₁₉H₂₇NO₃
• Molecular Weight: 317.428
• Mol file: 1163138-26-8.mol

Synonyms:

Chemical Property of (S)-N-benzyl-4-acetoxy-cis-7-decenamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-N-benzyl-4-acetoxy-cis-7-decenamide

There total 2 articles about (S)-N-benzyl-4-acetoxy-cis-7-decenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + rac-N-benzyl-4-hydroxy-cis-7-decenamide (259675-60-0) → (S)-N-benzyl-4-acetoxy-cis-7-decenamide (1163138-26-8) + (R)-N-benzyl-4-hydroxy-cis-7-decenamide

Guidance literature:

With Novozym 435; In diethyl ether; at 20 ℃; for 8h; optical yield given as %ee; Enzymatic reaction;

DOI:10.1080/00397910802546177

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + rac-N-benzyl-4-hydroxy-cis-7-decenamide (259675-60-0) + 4-nitro-benzoic acid (62-23-7) → (S)-N-benzyl-4-acetoxy-cis-7-decenamide (1163138-26-8) + (S)-N-benzyl-4-(4-nitrobenzoyl)oxy-cis-7-decenamide (1163138-32-6)

Guidance literature:

vinyl acetate; rac-N-benzyl-4-hydroxy-cis-7-decenamide; With Novozym 435; In diethyl ether; at 20 ℃; Enzymatic reaction;

4-nitro-benzoic acid; With di-isopropyl azodicarboxylate; triphenylphosphine; In benzene; at 20 ℃; for 48h; optical yield given as %ee;

DOI:10.1080/00397910802546177

upstream raw materials:

vinyl acetate

rac-N-benzyl-4-hydroxy-cis-7-decenamide

4-nitro-benzoic acid