((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph)

Base Information

Chemical Name:((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph)
CAS No.:929806-72-4
Molecular Formula:C₄₂H₈₆BCl₂O₃Si₃Ta
Molecular Weight:986.064
Hs Code.:

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Chemical Property of ((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph)

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Technology Process of ((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph)

There total 1 articles about ((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 104092-13-9
(t-Bu₃SiO)3Ta

: 873-51-8
phenylborondichloride

: 929806-72-4
((t)Bu3SiO)3Ta(η2-B,Cl-BCl2Ph)

Guidance literature:: In toluene; Ta compd. placed into a two-neck flask, a sidearm addn. tube charged with C6H5BCl2, cooled and evacuated, toluene added at -78°C, warmed to 23°C, C6H5BCl2 washed into the flask by condensing toluene, reacted for 1 h; filtered, concd., cooled to -78°C, pptd. (hexane), filtered, washed (cold hexane); elem. anal.;
DOI:10.1021/ic0616885