C₁₄H₁₄FN₃

Base Information

• Chemical Name: C₁₄H₁₄FN₃
• CAS No.: 1567436-92-3
• Molecular Formula: C₁₄H₁₄FN₃
• Molecular Weight: 243.284
• Mol file: 1567436-92-3.mol

Synonyms:

Chemical Property of C₁₄H₁₄FN₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₄FN₃

There total 3 articles about C₁₄H₁₄FN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H12FN3O2 (1567437-53-9) → C14H14FN3 (1567436-92-3)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol;

DOI:10.1016/j.bmcl.2014.01.001

Reference yield:

3-(3-nitrophenyl)azetidine (1567439-04-6) → C14H14FN3 (1567436-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 - 120 °C

2: hydrogen; palladium 10% on activated carbon / ethanol

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2014.01.001

Reference yield:

2,4-difluoropyridine (34941-90-7) → C14H14FN3 (1567436-92-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 - 120 °C

2: hydrogen; palladium 10% on activated carbon / ethanol

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2014.01.001

upstream raw materials:

C₁₄H₁₂FN₃O₂

3-(3-nitrophenyl)azetidine

2,4-difluoropyridine

Downstream raw materials:

C₂₆H₂₀FN₅O₂