(3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one

Base Information

Chemical Name:(3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one
CAS No.:17009-03-9
Molecular Formula:C29H41 N O4
Molecular Weight:467.649
Hs Code.:

Synonyms:Jervine,N-acetyl- (6CI,8CI); Veratraman-11-one, 28-acetyl-17,23-epoxy-3-hydroxy-, (3b,23b)-; N-Acetyljervine

Suppliers and Price of (3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one

Chemical Property:

Vapor Pressure:6.64E-20mmHg at 25°C
Boiling Point:654.5°C at 760 mmHg
Flash Point:349.6°C
Density:1.21g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one

There total 14 articles about (3beta,22S,23R)-28-acetyl-3-hydroxy-17,23-epoxyveratraman-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17008-94-5
(23R)-17,23-epoxy-(5α,13βH)-veratrane-3β,13-diol

: 17009-03-9
N-acetyljervine

Guidance literature:: Multi-step reaction with 9 steps

1: (acetylation)

2: SOCl₂, Py

3: CrO₃ / pyridine

4: (hydrolysis)

5: CrO₃ / dimethylformamide

6: DDQ

7: H₂ / Pd

8: (acetylation)

9: NaBH₄

With pyridine; chromium(VI) oxide; sodium tetrahydroborate; thionyl chloride; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/ja00993a048

Reference yield:

: 17008-98-9
(23R)-28-acetyl-17,23-epoxy-3β-hydroxy-(5α)-veratr-12-en-11-one

: 17009-03-9
N-acetyljervine

Guidance literature:: Multi-step reaction with 5 steps

1: CrO₃ / dimethylformamide

2: DDQ

3: H₂ / Pd

4: (acetylation)

5: NaBH₄

With chromium(VI) oxide; sodium tetrahydroborate; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium; In N,N-dimethyl-formamide;
DOI:10.1021/ja00993a048

Reference yield:

: 17008-95-6
(23R)-3β-acetoxy-28-acetyl-17,23-epoxy-(5α)-veratr-12-ene

: 17009-03-9
N-acetyljervine

Guidance literature:: Multi-step reaction with 7 steps

1: CrO₃ / pyridine

2: (hydrolysis)

3: CrO₃ / dimethylformamide

4: DDQ

5: H₂ / Pd

6: (acetylation)

7: NaBH₄

With chromium(VI) oxide; sodium tetrahydroborate; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/ja00993a048