C₂₇H₂₄O₃P₂

Base Information

• Chemical Name: C₂₇H₂₄O₃P₂
• CAS No.: 1454372-39-4
• Molecular Formula: C₂₇H₂₄O₃P₂
• Molecular Weight: 458.433
• Mol file: 1454372-39-4.mol

Synonyms:

Chemical Property of C₂₇H₂₄O₃P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₄O₃P₂

There total 4 articles about C₂₇H₂₄O₃P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichlorophenylphosphine (644-97-3) → C27H24O3P2 (1454372-39-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: diethyl ether / 16 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

2.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 0 - 20 °C / Schlenk technique; Inert atmosphere

2.2: 16 h / Schlenk technique; Inert atmosphere

3.1: water; hydrogenchloride / 1 h / Schlenk technique; Inert atmosphere

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; In diethyl ether; hexane;

DOI:10.1002/chem.201302230

Reference yield:

(diethylamino)phenylchlorophosphine (4073-31-8) → C27H24O3P2 (1454372-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 0 - 20 °C / Schlenk technique; Inert atmosphere

1.2: 16 h / Schlenk technique; Inert atmosphere

2.1: water; hydrogenchloride / 1 h / Schlenk technique; Inert atmosphere

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; water; In diethyl ether; hexane;

DOI:10.1002/chem.201302230

Reference yield:

C35H42N2OP2 (1158248-46-4) → C27H24O3P2 (1454372-39-4)

Guidance literature:

With hydrogenchloride; water; for 1h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201302230

upstream raw materials:

Dichlorophenylphosphine

(diethylamino)phenylchlorophosphine

C₃₅H₄₂N₂OP₂

9,9-dimethylxanthene

Downstream raw materials:

C₂₇H₂₂Cl₂OP₂

N,N'-((9,9-dimethyl-9H-xanthene-4,5-diyl)bis(phenylphosphinediyl))bis(4-butylbenzenesulfonamide)