C₁₁H₂₂N₂O₃

Base Information

Chemical Name:C₁₁H₂₂N₂O₃
CAS No.:1415794-22-7
Molecular Formula:C₁₁H₂₂N₂O₃
Molecular Weight:230.307
Hs Code.:

C<sub>11</sub>H<sub>22</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₂₂N₂O₃

Chemical Property:

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Technology Process of C₁₁H₂₂N₂O₃

There total 3 articles about C₁₁H₂₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415794-20-5,1228600-46-1
(S)-tert-butyl 2-acetylmorpholine-4-carboxylate

: 1415794-22-7,1824327-48-1
C₁₁H₂₂N₂O₃

Guidance literature:: With methanol; ammonium acetate; sodium cyanoborohydride; at 2 ℃; for 16h; Molecular sieve; Inert atmosphere;

Reference yield:

: 868689-63-8
(S)-2,4-morpholinedicarboxylic acid 4-(1,1-dimethylethyl)ester

: 1415794-22-7,1824327-48-1
C₁₁H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

2: tetrahydrofuran; diethyl ether / 17 h / 0 - 20 °C / Inert atmosphere

3: ammonium acetate; sodium cyanoborohydride; methanol / 16 h / 2 °C / Molecular sieve; Inert atmosphere

With methanol; ammonium acetate; sodium cyanoborohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 868689-64-9
(S)-2-(methoxy-methyl-carbamoyl)-morpholine-4-carboxylic acid tert-butyl ester

: 1415794-22-7,1824327-48-1
C₁₁H₂₂N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / 17 h / 0 - 20 °C / Inert atmosphere

2: ammonium acetate; sodium cyanoborohydride; methanol / 16 h / 2 °C / Molecular sieve; Inert atmosphere

With methanol; ammonium acetate; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether;